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褰撳墠浣嶇疆錛?棣栭〉 >> 璧勮 >> 澶嶅悎鏉愭枡 >> 琛屼笟鍔ㄦ?/a> >> 姝ｆ枃

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鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>娑?/span>鍙?/span>鏃?/span>鏈?/span>鎴?/span>鏈?/span>鏈?/span>鍗?/span>瀵?/span>浣?/span>銆?/span>閲?/span>灞?/span>銆?/span>灝?/span>瑁?/span>鏉?/span>鏂?/span>鍜?/span>鍩?/span>搴?/span>鏉?/span>鏂?/span>銆?/span>瑕?/span>鎯?/span>褰?/span>搴?/span>姣?/span>鍧?/span>寰?/span>鑺?/span>鐗?/span>錛?/span>鏈濂?/span>鐨?/span>鍔?/span>娉?/span>灝?/span>鏄?/span>璁?/span>榪?/span>浜?/span>鏉?/span>鏂?/span>娑?/span>澶?/span>銆?/span>縐?/span>瀛?/span>瀹?/span>浠?/span>瀵?/span>浜?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>鐨?/span>鐮?/span>絀?/span>灝?/span>涓?/span>瑕?/span>闆?/span>涓?/span>鍦?/span>鏉?/span>鏂?/span>鐨?/span>澶?/span>鏁?/span>妯?/span>寮?/span>鍜?/span>瑙?/span>鍙?/span>鏈?/span>鍒?/span>涓?/span>錛?/span>騫?/span>鍙?/span>寰?/span>浜?/span>涓浜?/span>寰?/span>濂?/span>鐨?/span>鎴?/span>鏋?/span>銆?/span>鐒?/span>鑰?/span>錛?/span>鐜?/span>鏈?/span>鐮?/span>絀?/span>涓?/span>鐨?/span>澶?/span>澶?/span>鏁?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>涓?/span>閮?/span>瀛?/span>鍦?/span>涓?/span>涓?/span>涓?/span>瑕?/span>闂?/span>棰?/span>銆?/span>絎?/span>涓錛?/span>榪?/span>浜?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>鐨?/span>緇?/span>鏋?/span>鍜?/span>鏉?/span>鏂?/span>鍗?/span>鍒?/span>鐗?/span>孌?/span>錛?/span>涓?/span>鐜?/span>鏈?/span>鐨?/span>浜?/span>琛?/span>閲?/span>灞?/span>姘?/span>鍖?/span>鐗?/span>鍗?/span>瀵?/span>浣?/span>(CMOS)鍜?/span>闆?/span>鎴?/span>鐢?/span>璺?/span>(IC)鐨?/span>鍒?/span>閫?/span>宸?/span>鑹?/span>鍜?/span>鎶鏈?/span>涓?/span>鍏?/span>瀹?/span>銆?/span>絎?/span>浜?/span>錛?/span>榪?/span>浜?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>澶?/span>鏁?/span>鏃?/span>闂?/span>杈?/span>闀?/span>錛?/span>鏈?/span>鐨?/span>鐢?/span>鑷?/span>闀?/span>杈?/span>鏁?/span>騫?/span>錛?/span>榪?/span>灝?/span>闄?/span>鍒?/span>浜?/span>榪?/span>浜?/span>鎶鏈?/span>鍦?/span>鏁?/span>鎹?/span>瀹?/span>鍏?/span>鏂?/span>闈?/span>鐨?/span>搴?/span>鐢?/span>銆?/span>涓?/span>浜?/span>騫?/span>娉?/span>瀹?/span>鐜?/span>淇?/span>鎭?/span>瀹?/span>鍏?/span>錛?/span>闄?/span>浣?/span>鏁?/span>鎹?/span>娉?/span>闇?/span>鐨?/span>椋?/span>闄?/span>錛?/span>鍏?/span>瀹?/span>鐨?/span>鍒?/span>閫?/span>宸?/span>鑹?/span>鍜?/span>蹇?/span>閫?/span>鐨?/span>鑷?/span>姣?/span>鑳?/span>鍔?/span>鏄?/span>鑷?/span>鍏?/span>閲?/span>瑕?/span>鐨?/span>銆?/span>


鍩?/span>浜?/span>浠?/span>涓?/span>鑳?/span>鏅?/span>錛?/span>浠?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>(EMs)涓?/span>宸?/span>浣?/span>浠?/span>璐?/span>鐨?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>灝?/span>鍏?/span>鏈?/span>紿?/span>鍑?/span>鐨?/span>浼?/span>鍔?/span>銆?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>涓?/span>浠?/span>鍖?/span>瀛?/span>鑳?/span>鐨?/span>褰?/span>寮?/span>鍌?/span>瀛?/span>鏈?/span>澶?/span>閲?/span>鑳?/span>閲?/span>錛?/span>鍦?/span>澶?/span>鐣?/span>鍒?/span>嬋涓?/span>錛?/span>榪?/span>浜?/span>鑳?/span>閲?/span>鍙?/span>浠?/span>琚?/span>榪?/span>閫?/span>閲?/span>鏀?/span>鍑?/span>鏉?/span>銆?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>鍏?/span>鏈?/span>瑙?/span>鍙?/span>鍙?/span>鎺?/span>銆?/span>鑳?/span>閲?/span>閲?/span>鏀?/span>蹇?/span>銆?/span>鐮?/span>鍧?/span>鎬?/span>寮?/span>絳?/span>鐗?/span>鐐?/span>錛?/span>鏈?/span>鏈?/span>婊?/span>瓚?/span>鐬?/span>鎬?/span>寰?/span>鑺?/span>鐗?/span>鐨?/span>闇姹?/span>銆?/span>鐒?/span>鑰?/span>錛?/span>瑕?/span>鎯?/span>鍦?/span>寰?/span>綰?/span>綾?/span>灝?/span>搴?/span>涓?/span>鍚?/span>鏃?/span>瀹?/span>鐜?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>鐨?/span>鍙?/span>闈?/span>鐐?/span>鐏?/span>銆?/span>鑷?/span>鎸?/span>鐕?/span>鐑?/span>銆?/span>鐮?/span>鍧?/span>鏁?/span>鑳?/span>銆?/span>浠?/span>鍙?/span>涓?/span>寰?/span>鍣?/span>浠?/span>闆?/span>鎴?/span>錛?/span>浠?/span>闈?/span>涓?/span>鐫宸?/span>澶?/span>鎸?/span>鎴?/span>錛?/span>鍥?/span>姝?/span>瀵?/span>鎵?/span>鍚?/span>閫?/span>鐨?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>宸?/span>浣?/span>浠?/span>璐?/span>鍜?/span>鍏?/span>瀹?/span>鐨?/span>闆?/span>鎴?/span>鏂?/span>娉?/span>瀵?/span>浜?/span>瀹?/span>鐜?/span>寰?/span>鑺?/span>鐗?/span>鐨?/span>鐬?/span>鏃?/span>鑷?/span>姣?/span>鑷?/span>鍏?/span>閲?/span>瑕?/span>銆?/span>


鍦?/span>涔?/span>鍓?/span>鐨?/span>鐮?/span>絀?/span>涓?/span>錛?/span>璇?/span>璇?/span>棰?/span>緇?/span>鍙?/span>鐜?/span>浠?/span>閲?/span>灞?/span>涓?/span>蹇?/span>鍜?/span>瀵?/span>姘?/span>鏈?/span>鏈?/span>閰?/span>浣?/span>鏋?/span>寤?/span>鐨?/span>寰?/span>綾?/span>綰?/span>鍚?/span>鑳?/span>閰?/span>浣?/span>鑱?/span>鍚?/span>鐗?/span> (ECPs) 涓?/span>綰?/span>綾?/span>閾?/span>綺?/span>娣?/span>鍚?/span>鍚?/span>鍏?/span>鏈?/span>浼?/span>寮?/span>鐨?/span>鐕?/span>鐑?/span>鍜?/span>浜?/span>鍘?/span>鑳?/span>鍔?/span>錛?/span>騫?/span>鍙?/span>浠?/span>閫?/span>榪?/span>鐒?/span>鑰?/span>鍔?/span>鐑?/span>鐐?/span>鐕?/span>銆?/span>鐒?/span>鑰?/span>寰?/span>綾?/span>綰?/span>ECPs鐨?/span>涓?/span>鐣?/span>灝?/span>瀵?/span>榪?/span>澶?/span>錛?/span>涓?/span>鍒?/span>浜?/span>寰?/span>灝?/span>搴?/span>涓?/span>鐕?/span>鐑?/span>鐨?/span>浼?/span>鎾?/span>錛?/span>涓?/span>鍏?/span>綺?/span>鏈?/span>褰?/span>鎬?/span>涓?/span>鑳?/span>涓?/span>寰?/span>鍔?/span>鐑?/span>鍣?/span>闆?/span>鎴?/span>銆?/span>涓?/span>浜?/span>瑙?/span>鍐?/span>榪?/span>浜?/span>闂?/span>棰?/span>錛?/span>鍏?/span>鍒?/span>鍙?/span>鎸?/span>ECPs鐨?/span>浼?/span>鍔?/span>錛?/span>璇?/span>璇?/span>棰?/span>緇?/span>璁?/span>鍒?/span>灝?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>(GO)寮?/span>鍏?/span>ECPs鐨?/span>閰?/span>浣?/span>鍜?/span>緇?/span>鏅?/span>榪?/span>紼?/span>涓?/span>錛?/span>鍥?/span>涓?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鏈?/span>鍥?/span>澶?/span>浼?/span>鐐?/span>錛?/span>1錛?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鏈?/span>韜?/span>鏄?/span>涓縐?/span>鍚?/span>鑳?/span>鏉?/span>鏂?/span>錛?/span>鍏?/span>鍚?/span>姘?/span>鍩?/span>鍥?/span>鍦?/span>200?小宸?/span>鍙?/span>鍒?/span>瑙?/span>騫?/span>閲?/span>鏀?/span>澶?/span>閲?/span>鐑?/span>閲?/span>錛?/span>2錛?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鐗?/span>灞?/span>涓?/span>鐨?/span>緹?/span>鍩?/span>鍏?/span>鏈?/span>涓?/span>閲?/span>灞?/span>紱?/span>瀛?/span>閰?/span>浣?/span>鐨?/span>鑳?/span>鍔?/span>錛?/span>浠?/span>鑰?/span>璇?/span>瀵?/span>ECPs鍦?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鐗?/span>灞?/span>涓?/span>鍘?/span>浣?/span>鐢?/span>闀?/span>錛?/span>3錛?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鐨?/span>灞?/span>鐘?/span>緇?/span>鏋?/span>鍏?/span>鏈?/span>絀?/span>闂?/span>綰?/span>鏉?/span>鏁?/span>搴?/span>錛?/span>鍙?/span>浠?/span>鍑?/span>灝?/span>ECPs鏅?/span>浣?/span>鐨?/span>灝?/span>瀵?/span>錛?/span>4錛?/span>浣?/span>涓?/span>涓縐?/span>浜?/span>緇?/span>鏉?/span>鏂?/span>錛?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>涓?/span>灞?/span>涔?/span>闂?/span>浠?/span>鍙?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>涓?/span>鍩?/span>搴?/span>涔?/span>闂?/span>瀛?/span>鍦?/span>鑼?/span>寰?/span>鍗?/span>鍔?/span>錛?/span>浠?/span>鑰?/span>鏈?/span>鍒?/span>浜?/span>鏉?/span>鏂?/span>鍦?/span>鍩?/span>搴?/span>涓?/span>鐨?/span>鑷?/span>鐒?/span>鎴?/span>鑶?/span>鍜?/span>绱?/span>瀵?/span>緇?/span>鍚?/span>銆?/span>


鎹?/span>姝?/span>錛?/span>璇?/span>璇?/span>棰?/span>緇?/span>鎴?/span>鍔?/span>鍦?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鐗?/span>灞?/span>涓?/span>寮?/span>鍏?/span>1,1鈥?/span>-浜?/span>緹?/span>鍩?/span>-5,5鈥?/span>-鑱?/span>鍥?/span>鍞?/span>錛?/span>H2BTO錛?/span>涓?/span>閽?/span>紱?/span>瀛?/span>閰?/span>浣?/span>褰?/span>鎴?/span>鐨?/span>綰?/span>綾?/span>ECPs錛?/span>騫?/span>閫?/span>榪?/span>婊?/span>閾?/span>娉?/span>鍦?/span>鐢?/span>闃?/span>寮?/span>寰?/span>鍔?/span>鐑?/span>鍣?/span>涓?/span>鍒?/span>澶?/span>鍑?/span>鍏?/span>鏈?/span>鑹?/span>濂?/span>緇?/span>鍚?/span>鍔?/span>鐨?/span>GO-ECP(Co)鍚?/span>鑳?/span>钖?/span>鑶?/span>銆?/span>璇?/span>璇?/span>棰?/span>緇?/span>璇?/span>緇?/span>鐮?/span>絀?/span>浜?/span>GO-ECP(Co)鍚?/span>鑳?/span>钖?/span>鑶?/span>鐨?/span>緇?/span>鏋?/span>褰?/span>鎴?/span>鏈?/span>鐞?/span>鍜?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鍚?/span>閲?/span>瀵?/span>鍚?/span>鑳?/span>鐗?/span>鎬?/span>鐨?/span>褰?/span>鍝?/span>錛?/span>榪?/span>琛?/span>浜?/span>璺?/span>钀?/span>嫻?/span>璇?/span>浠?/span>璇?/span>鏄?/span>鍚?/span>鑳?/span>钖?/span>鑶?/span>涓?/span>紜?/span>鍩?/span>搴?/span>鐨?/span>寮?/span>緇?/span>鍚?/span>鍔?/span>銆?/span>鏇?/span>閲?/span>瑕?/span>鐨?/span>鏄?/span>錛?/span>0.1mg璇?/span>鍚?/span>鑳?/span>钖?/span>鑶?/span>涓?/span>紺?/span>渚?/span>鑺?/span>鐗?/span>灝?/span>瑁?/span>鍚?/span>錛?/span>鍙?/span>鍦?/span>1s鍐?/span>浣?/span>鍏?/span>褰?/span>搴?/span>綺?/span>紕?/span>銆?/span>


A. 綰?/span>綾?/span>GO-ECP(Co)鐨?/span>褰?/span>鎴?/span>


褰?/span>婧?/span>娑?/span>涓?/span>鍙?/span>鏈?/span>Co2 鍜?/span>H2BTO閰?/span>浣?/span>鏃?/span>錛?/span>閰?/span>浣?/span>鍜?/span>鑱?/span>鍚?/span>鍙?/span>搴?/span>榪?/span>閫?/span>鍙?/span>鐢?/span>錛?/span>褰?/span>鎴?/span>寰?/span>綾?/span>綰?/span>鐨?/span>ECP (Co)鏅?/span>浣?/span>銆?/span>鐒?/span>鑰?/span>錛?/span>褰?/span>鏅?/span>浣?/span>鐢?/span>闀?/span>榪?/span>紼?/span>鍙?/span>鐢?/span>鍦?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>闂?/span>鏃?/span>錛?/span>鐢?/span>浜?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>闂?/span>鐨?/span>絀?/span>闂?/span>闄?/span>鍩?/span>鏁?/span>搴?/span>錛?/span>綰?/span>綾?/span>灝?/span>搴?/span>鐨?/span>ECP (Co)灝?/span>濉?/span>鍏?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>闂?/span>銆?/span>


Figure 1. Schematic illustration for the synthesis of nano GO-ECP(Co). GO plays a key role in reducing the size of ECP(Co).


B. GO-ECP(Co)鐨?/span>褰?/span>璨?/span>


綰?/span>ECP(Co)棰?/span>綺?/span>鍛?/span>寰?/span>綾?/span>綰?/span>鐨?/span>鍗?/span>瀛?/span>褰?/span>鐘?/span>錛?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>涓?/span>鐨?/span>ECP(Co)棰?/span>綺?/span>鍒?/span>鍛?/span>綰?/span>綾?/span>綰?/span>鐨?/span>綰?/span>閿?/span>褰?/span>鐘?/span>銆?/span>緇?/span>鐪?/span>絀?/span>鎶?/span>婊?/span>鍚?/span>錛?/span>GO-ECP(Co)鍙?/span>浠?/span>褰?/span>鎴?/span>瀹?/span>鏁?/span>鐨?/span>钖?/span>鑶?/span>銆?/span>璇?/span>钖?/span>鑶?/span>涓?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>钖?/span>鑶?/span>鐩?/span>姣?/span>錛?/span>琛?/span>闈?/span>鍜?/span>鎴?/span>闈?/span>SEM鍥?/span>涓?/span>鍧?/span>鏄?/span>鏄?/span>瀛?/span>鍦?/span>澶?/span>閲?/span>瀵?/span>闆?/span>鐨?/span>GO-ECP(Co)棰?/span>綺?/span>銆?/span>


Figure 2. The SEM images of ECP(Co) powder (a), GO-ECP(Co) energetic film with 7.5 wt% GO content (b) and GO/ECP(Co) mixture with 5 wt% GO content(c); TEM image (d), HAADF-STEM image (i) and corresponding elemental mapping results (e-h) of GO-ECP(Co) dispersion with 7.5 wt% GO content; The picture of GO-ECP(Co) energetic film with 7.5 wt% GO content is obtained from vacuum filtration and drying (j); The top-view SEM image of GO film (k); The cross-view SEM images of GO film (l) and GO-ECP(Co) energetic film with 7.5 wt% GO content (m).


C. 姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>涓?/span>Co2 紱?/span>瀛?/span>涔?/span>闂?/span>鐨?/span>浣?/span>鐢?/span>鍜?/span>ECP(Co)灝?/span>瀵?/span>鍑?/span>灝?/span>鐨?/span>鍘?/span>鍥?/span>


XPS鍜?/span>FTIR琛?/span>寰?/span>璇?/span>瀹?/span>浜?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>鐨?/span>-COOH鍩?/span>鍥?/span>涓?/span>Co2 紱?/span>瀛?/span>涔?/span>闂?/span>瀛?/span>鍦?/span>閰?/span>浣?/span>鍏?/span>浠?/span>閿?/span>錛?/span>榪?/span>縐?/span>閰?/span>浣?/span>鏁?/span>搴?/span>浣?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>灞?/span>涓?/span>ECP(Co)棰?/span>綺?/span>绱?/span>瀵?/span>緇?/span>鍚?/span>銆?/span>XRD鍥?/span>璋?/span>涓?/span>GO-ECP (Co)鐨?/span>鐗?/span>寰?/span>琛?/span>灝?/span>宄?/span>涓?/span>綰?/span>ECP(Co)鐩?/span>姣?/span>錛?/span>鍗?/span>楂?/span>瀹?/span>鏄?/span>鏄?/span>澧?/span>澶?/span>錛?/span>琛?/span>鏄?/span>鏅?/span>浣?/span>灝?/span>瀵?/span>鍑?/span>灝?/span>銆?/span>GO-ECP (Co)浣?/span>浜?/span>16.4?澶?/span>鐨?/span>琛?/span>灝?/span>宄?/span>涓?/span>鍏?/span>浣?/span>鐨?/span>琛?/span>灝?/span>宄?/span>鐨?/span>鐩?/span>瀵?/span>寮?/span>搴?/span>涓?/span>綰?/span>ECP(Co)鐩?/span>姣?/span>鏄?/span>钁?/span>澧?/span>鍔?/span>錛?/span>璇?/span>鏄?/span>GO-ECP (Co)鏅?/span>浣?/span>涓?/span>瑕?/span>娌?/span>涓涓?/span>鏅?/span>闈?/span>鐢?/span>闀?/span>錛?/span>鍏?/span>浣?/span>鏅?/span>闈?/span>涓?/span>鐨?/span>鐢?/span>闀?/span>鍙?/span>鍒?/span>鎶?/span>鍒?/span>錛?/span>瀵?/span>鑷?/span>灝?/span>瀵?/span>鍑?/span>灝?/span>銆?/span>


Figure 3. XPS survey spectra between 0 and 900 eV (a), high resolution XPS spectra for O1s (b) and FTIR spectra (insert is the pictures of GO, GO/H2BTO ligand, GO-Co and GO-ECP(Co) with 7.5 wt% GO content in deionized water) (c) of GO and GO-Co complex; XRD patterns of ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) energetic film with 7.5 wt% GO content (d).


D. GO-ECP(Co)鐨?/span>鍚?/span>鑳?/span>鐗?/span>鎬?/span>


TG-DSC鍒?/span>鏋?/span>鏄?/span>紺?/span>GO-ECP(Co)涓?/span>ECP(Co)鐩?/span>姣?/span>鍏?/span>鏈?/span>杈?/span>濂?/span>鐨?/span>鐑?/span>紼?/span>瀹?/span>鎬?/span>銆?/span>杈?/span>澶?/span>鐨?/span>鏀?/span>鐑?/span>閲?/span>鍜?/span>杈?/span>楂?/span>鐨?/span>鑳?/span>閲?/span>閲?/span>鏀?/span>閫?/span>鐜?/span>銆?/span>瀵?/span>闂?/span>鑵?/span>浣?/span>涓?/span>鐨?/span>浜?/span>鍘?/span>瀹?/span>楠?/span>璇?/span>鏄?/span>鍦?/span>鍚?/span>鏍?/span>鐨?/span>瀹?/span>楠?/span>鏉?/span>浠?/span>涓?/span>錛?/span>GO-ECP(Co)鍏?/span>鏈?/span>榪?/span>楂?/span>浜?/span>ECP(Co)鐨?/span>鍘?/span>鍔?/span>宄?/span>鍊?/span>鍜?/span>澧?/span>鍘?/span>閫?/span>鐜?/span>銆?/span>寮鏀?/span>鐜?/span>澧?/span>涓?/span>鐨?/span>鐐?/span>鐏?/span>瀹?/span>楠?/span>璇?/span>鏄?/span>鍦?/span>鍚?/span>鏍?/span>鐨?/span>瀹?/span>楠?/span>鏉?/span>浠?/span>涓?/span>錛?/span>GO-ECP(Co)鍏?/span>鏈?/span>榪?/span>浼?/span>浜?/span>ECP(Co)鐨?/span>鐕?/span>鐑?/span>鎬?/span>鑳?/span>錛?/span>鍙?/span>浠?/span>鍙?/span>鐢?/span>鑷?/span>鎸?/span>鐕?/span>鐑?/span>錛?/span>涓?/span>娌?/span>鏈?/span>鍓?/span>浣?/span>鐨?/span>鏈?/span>鍙?/span>搴?/span>鏍?/span>鍝?/span>銆?/span>


Figure 4. TG and DSC curves of pure ECP(Co) and GO-ECP(Co) composite (7.5 wt% GO content) at Ar atmosphere from 60?C to 750 ?C with a heating rate of 10 ?C/min (a). Dynamic pressure curves of pure ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) composite (7.5 wt% GO content) in pressure-generation experiments at closed environment (inset is a schematic cross-sectional view of the experimental apparatus) (b). Burning sequences of pure ECP(Co), GO/ECP(Co) mixture and GO-ECP(Co) composite (7.5 wt% GO content) in burning experiments at open environment (inset is a schematic cross-sectional view of the sample container) (c).


E. GO-ECP(Co)钖?/span>鑶?/span>涓?/span>鍩?/span>搴?/span>鐨?/span>寮?/span>緇?/span>鍚?/span>鑳?/span>鍔?/span>



Figure 5. Photos of the prepared GO-ECP(Co) energetic films with 7.5 wt% GO content on a silicon wafer before and after demolding (total mass of the four films is 1.5 mg) (a). Photos of the energetic film on the silicon wafer before and after falling from a height of 10cm (b), 30cm (c) and 50cm (d), respectively.


F. 寰?/span>鑺?/span>鐗?/span>鐨?/span>鐬?/span>鎬?/span>鎬?/span>鑳?/span>


鍦?/span>Au/Pt/Cr寰?/span>鍔?/span>鐑?/span>鍣?/span>鐨?/span>鐢?/span>闃?/span>鍖?/span>鍩?/span>婊?/span>閾?/span>GO-ECP(Co)钖?/span>鑶?/span>錛?/span>鐒?/span>鍚?/span>灝?/span>瑁?/span>鍦?/span>200渭m鍘?/span>鐨?/span>紜?/span>鍩?/span>鑺?/span>鐗?/span>涓?/span>銆?/span>緇?/span>寰?/span>鍔?/span>鐑?/span>鍣?/span>涓?/span>绔?/span>閫?/span>鐢?/span>鍚?/span>錛?/span>鐢?/span>浜?/span>鐒?/span>鑰?/span>鍔?/span>鐑?/span>錛?/span>寰?/span>鍔?/span>鐑?/span>鍣?/span>鐢?/span>闃?/span>鍖?/span>娓?/span>搴?/span>鍗?/span>楂?/span>銆?/span>褰?/span>娓?/span>搴?/span>涓?/span>鍗?/span>鍒?/span>鍚?/span>鑳?/span>鑳?/span>钖?/span>鑶?/span>鐨?/span>鐐?/span>鐏?/span>娓?/span>搴?/span>鏃?/span>錛?/span>鍏?/span>鏀?/span>鐑?/span>鍙?/span>搴?/span>琚?/span>瑙?/span>鍙?/span>錛?/span>閲?/span>鏀?/span>鍑?/span>澶?/span>閲?/span>鐨?/span>鐑?/span>閲?/span>鍜?/span>姘?/span>浣?/span>錛?/span>浜?/span>鐢?/span>灞閮?/span>楂?/span>娓?/span>楂?/span>鍘?/span>錛?/span>浠?/span>鑰?/span>鐮?/span>鍧?/span>紜?/span>鍩?/span>鑺?/span>鐗?/span>銆?/span>0.1mg鐨?/span>GO鍚?/span>閲?/span>涓?/span>7.5 wt%鐨?/span>GO-ECP(Co)钖?/span>鑶?/span>涓?/span>鐨?/span>紜?/span>鍩?/span>鑺?/span>鐗?/span>鍦?/span>鏀?/span>鐑?/span>鍙?/span>搴?/span>瑙?/span>鍙?/span>鍚?/span>4ms鍐?/span>琚?/span>綺?/span>紕?/span>銆?/span>鏁?/span>涓?/span>鑷?/span>姣?/span>榪?/span>紼?/span>鍦?/span>1s鍐?/span>瀹?/span>鎴?/span>銆?/span>


Figure 6. The microscope photographs of Au/Pt/Cr microheater on a glass substrate (a), GO-ECP(Co) energetic film with 7.5 wt% GO content (about 0.1mg) on the microheater (b), transient microchip consisting of a silicon chip, energetic film and microheater (c) and transient microchip after self-destruction (d), photo sequence of the self-destruction process of the transient microchip captured by a high-speed camera (e), typical volt-ampere dynamic curves of the microheater during the test of transient performance (f).


鎬?/span>緇?/span>涓?/span>灞?/span>鏈?/span>


璇?/span>璇?/span>棰?/span>緇?/span>寮鍙?/span>浜?/span>涓縐?/span>鍩?/span>浜?/span>姘?/span>鍖?/span>鐭?/span>澧?/span>鐑?/span>-綰?/span>綾?/span>鍚?/span>鑳?/span>閰?/span>浣?/span>鑱?/span>鍚?/span>鐗?/span>鐨?/span>鏂?/span>鍨?/span>綰?/span>綾?/span>鍚?/span>鑳?/span>钖?/span>鑶?/span>錛?/span>鍙?/span>鍦?/span>寰?/span>綰?/span>綾?/span>灝?/span>搴?/span>涓?/span>瀹?/span>鐜?/span>鍙?/span>闈?/span>鐐?/span>鐏?/span>銆?/span>鑷?/span>鎸?/span>鐕?/span>鐑?/span>銆?/span>寮?/span>鐮?/span>鍧?/span>鏁?/span>鑳?/span>錛?/span>騫?/span>鍙?/span>涓?/span>寰?/span>鍔?/span>鐑?/span>鍣?/span>闆?/span>鎴?/span>瀹?/span>鐜?/span>寰?/span>鑺?/span>鐗?/span>鐬?/span>鏃?/span>鑷?/span>姣?/span>銆?/span>


璇?/span>钖?/span>鑶?/span>闆?/span>浼?/span>縐鐨?/span>鏀?/span>鐑?/span>銆?/span>鐕?/span>鐑?/span>銆?/span>浜?/span>姘?/span>鎬?/span>鑳?/span>涓?/span>涓浣?/span>錛?/span>騫?/span>瀹?/span>鏄?/span>涓?/span>鍣?/span>浠?/span>琛?/span>闈?/span>緇?/span>鍚?/span>錛?/span>鏈?/span>鏉?/span>鍙?/span>鍦?/span>寰?/span>姘?/span>浣?/span>鎺?/span>榪?/span>鍣?/span>銆?/span>寰?/span>鐐?/span>鐏?/span>鍣?/span>銆?/span>寰?/span>椹?/span>鍔?/span>瑁?/span>緗?/span>絳?/span>寰?/span>綰?/span>鍣?/span>浠?/span>涓?/span>騫?/span>娉?/span>搴?/span>鐢?/span>銆?/span>


鐩?/strong>鍏?/strong>閾?/strong>鎺?/strong>

https://doi.org/10.1002/adfm.202103199

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