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褰撳墠浣嶇疆錛?棣栭〉 >> 璧勮 >> 澶嶅悎鏉愭枡 >> 琛屼笟鍔ㄦ?/a> >> 姝ｆ枃
  鐢變簬閾濋噾灞炲叿鏈夎祫婧愪赴瀵屻佹瘮瀹歸噺楂樹(shù)互鍙?qiáng)鎴愭湰浣幗{変紭鍔匡紝鍥犳閾濈數(shù)姹犳垚涓哄浠鋒侀噾灞炵數(shù)姹犵殑鐮旂┒鐑偣銆備絾鐩?/span>鍓嶅彲鍏呯數(shù)閾濈數(shù)姹犱富嫻佺數(shù)瑙ｈ川錛?/span>AlCl3鍩虹瀛愭恫浣擄級(jí)闈復(fù)鐨勪竴浜涘叧閿殑闂錛屽姘村垎鏁忔劅鎬с佺數(shù)瑙ｆ恫娉勯湶鍜岃厫铓絳夐樆紕嶄簡(jiǎn)閾濈數(shù)姹犵殑鍙戝睍銆?/span>


  灞變笢縐戞妧澶у鏋楀瓱鏄屻佹潨鎯犲鉤絳夊埄鐢ㄤ綆鎴愭湰AlCl3/Et3NHCl錛?/span>Et3NHCl錛氫笁涔欒兒鐩愰吀鐩愶級(jí)紱誨瓙娑蹭綋涓庤仛閰拌兒鐨勫嚌鑳跺寲浣滅敤錛岄氳繃綆鍗曠殑娣峰悎鏂規(guī)硶鍒跺浜?jiǎn)鏂板瀷鍑濊兌鑱氬悎鐗╃數(shù)瑙ｈ川銆傝鍑濊兌鑱氬悎鐗╃數(shù)瑙ｈ川鍦ㄥ娓╂潯浠朵笅琛ㄧ幇鍑?guó)櫨冮珮鐨劶浾d瓙鐢?shù)瀵肩巼锛?/span>3.86× 10-3 S cm-1錛夈佸鐢?shù)鍖栧绐楀彛锛?/span>2.6 V vs. Al錛夊強(qiáng)闀挎湡鐣岄潰紼沖畾鎬с傚彟澶栵紝涓庣瀛愭恫浣撶浉姣旓紝璇ュ嚌鑳惰仛鍚堢墿鐢?shù)瑙ｈ川琛ㄧ幇鍑鸿緝浣庣殑姘村垎鏁忔劅鎬у拰鑵愯殌鎬с傞噰鐢ㄨ鍑濊兌鑱氬悎鐗╃數(shù)瑙ｈ川緇勮鐨勯摑-鐭沖ⅷ鐢墊睜琛ㄧ幇鍑?guó)櫨冨ソ鐨勫嶇巼鎬ц兘銆佽緝闀跨殑寰幆鎬ц兘浠ュ強(qiáng)浼樺紓鐨勬姂鍒惰嚜鏀劇數(shù)鎬ц兘銆傝宸ヤ綔浠?/span>鈥淟ow-Cost Gel Polymer Electrolyte for High-Performance Aluminum-Ion Batteries鈥?/span>涓洪錛屽彂琛ㄤ簬銆?/span>ACS Applied Materials & Interfaces銆嬫湡鍒娿?/span>


1.鍑濊兌鐢?shù)瑙ｈ川鍩烘湰鎬ц川



鍥?/span>1.錛?/span>a錛変笂閮ㄥ垎涓?/span>AlCl3/Et3NHCl錛?/span>AT錛夌瀛愭恫浣擄紝涓嬮儴鍒嗕負(fù)AT鍩哄嚌鑳訛紱

錛?/span>b錛?/span>AT鍩虹瀛愭恫浣撲笌d鍑濊兌鎷夋浖鍥捐氨


  璇ュ嚌鑳惰仛鍚堢墿鐢?shù)瑙ｈ川鍒跺鏂规硶绠鍗曪紝鍙渶灝嗙瀛愭恫浣撲笌鑱氶叞鑳烘販鍚堬紝榪涜綆鍗曠殑鍔犵儹鎼呮媽鍗沖埗澶囦簡(jiǎn)鍥涚涓嶅悓姣斾緥鐨?/span>AlCl3/Et3NHCl鐨勫嚌鑳惰仛鍚堢墿鐢?shù)瑙ｈ川銆備粠鎷夋浖鍥捐氨鍙互鐪嬪嚭鍑濊兌涓庣瀛愭恫浣撶殑鏈夋晥鎴愬垎鏄竴鏍風(fēng)殑錛屽潎涓?/span>Al2Cl7-鍜?/span>AlCl4-闃寸瀛愶紝榪欒鏄庝笉鍚屽嚌鑳剁數(shù)瑙ｈ川鍧囧彲搴旂敤浜庨摑紱誨瓙鐢墊睜銆?/span>


  2.鍑濊兌鐢?shù)瑙ｈ川鐨勭數(shù)鍖栧鎬ц兘浠ュ強(qiáng)鐢墊睜鎬ц兘



鍥?/span>2.錛?/span>a錛変笉鍚屽嚌鑳惰仛鍚堢墿鐢?shù)瑙ｈ川鐢ㄤ簬閾?/span>-鐭沖ⅷ鐢墊睜鐨勫嶇巼鎬ц兘錛涳紙b錛変嬌鐢?/span>AT1.7 PA鍑濊兌鐢?shù)瑙ｈ川鐨勯?/span>-鐭沖ⅷ鐢墊睜鍦ㄤ笉鍚岀數(shù)嫻佸瘑搴︿笅鐨勫厖鏀劇數(shù)鏇茬嚎錛?/span>AT1.7 PA鐢?shù)瑙ｈ川鐨勫Q?/span>c錛?/span>LSV鏇茬嚎錛涳紙d錛夌瀛愮數(shù)瀵肩巼錛涳紙e錛夋亽嫻佹瀬鍖栨洸綰匡紱錛?/span>f錛変嬌鐢?/span>AT1.7 PA鍑濊兌鐢?shù)瑙ｈ川鐨勯?/span>-鐭沖ⅷ鐢墊睜鐨勯暱寰幆鎬ц兘


  閫氳繃瀵規(guī)瘮涓嶅悓鍑濊兌鑱氬悎鐗╃數(shù)瑙ｈ川鐢ㄤ簬閾?/span>-鐭沖ⅷ鐢墊睜鐨勫嶇巼鎬ц兘錛屽彲浠ョ湅鍑?/span>AT1.7 PA鐢?shù)瑙ｈ川鍦ㄦ瘮瀹归噺銆佸簱浼︽晥鐜囩瓑鏂歸潰鍧囪〃鐜板嚭浼樺紓鐨勬ц兘銆傚洜姝?/span>鏈枃鐫閲?/span>瀵?/span>AT1.7 PA鐢?shù)瑙ｈ川杩涜鐮斀I躲備粠AT1.7涓?/span>AT1.7 PA鐨?/span>LSV鏇茬嚎鍙互鐪嬪嚭錛?/span>AT1.7 PA鍏鋒湁涓?/span>AT1.7鐩稿綋鐨勭數(shù)鍖栧紿楀彛錛涘嚌鑳剁殑VTF鏂圭▼鎷熷悎鏄劇ず鍑?guó)櫨冧綆鐨?/span>紱誨瓙浼犺緭鑳介噺鍔垮瀿錛涘嚌鑳跺湪3800涓皬鏃剁殑鎭掓祦鏋佸寲涓〃鐜板嚭紼沖畾鐨勬瀬鍖栫數(shù)鍘嬶紝璇存槑鐣岄潰杈冪ǔ瀹氥傞噰鐢ㄨ鍑濊兌鐢?shù)瑙ｈ川缁勮鐨勯?/span>-鐭沖ⅷ鐢墊睜瀹ゆ俯鏉′歡涓嬬ǔ瀹氬驚鐜?/span>2000鍦堬紝浼樹(shù)簬涔嬪墠鏂囩尞鎶ラ亾鐨勫嚌鑳墮摑-鐭沖ⅷ鐢墊睜鐨勬ц兘銆?/span>


  3.閲囩敤鍑濊兌鐢?shù)瑙ｈ川鐨勯?/span>-鐭沖ⅷ鐢墊睜宸ヤ綔鏈虹悊


鍥?/span>3.閲囩敤鍑濊兌鐢?shù)瑙ｈ川鐨勯?/span>-鐭沖ⅷ鐢墊睜鐨勶紙a錛夊師浣?/span>XRD鍥捐氨錛涳紙b錛夊厖鏀劇數(shù)鏇茬嚎錛涳紙c錛夊師浣?/span>Raman鍥捐氨


  浠庣數(shù)姹犲師浣?/span>XRD鍥捐氨鍙?qiáng)鍘熶?/span>Raman鍥捐氨鍙互鐪嬪嚭錛屽湪姝ｆ瀬鍙戠敓鐨勬槸宓屽叆鍙嶅簲錛屼笌鏂囩尞涓姤閬撶殑紱誨瓙娑蹭綋閾?/span>-鐭沖ⅷ鐢墊睜鍙嶅簲涓鑷淬?/span>


  4.鍑濊兌鐢?shù)瑙ｈ川鐨勫姛鑳芥?/span>

鍥?/span>4.AT1.7涓?/span>AT1.7 PA鍒嗗埆鏆撮湶鍦ㄧ┖姘斾腑10鍒嗛挓鍚庯紙a錛夋矇縐憾瑙ｉ摑鐨?/span>CV鏇茬嚎錛涳紙b錛夌粍瑁呴摑-鐭沖ⅷ鐢墊睜鐨勫驚鐜ц兘


  浠?/span>CV鏇茬嚎鍙互鐪嬪嚭錛?/span>AT1.7鏆撮湶浜庣┖姘斿悗錛屽け鍘葷數(shù)鍖栧媧繪э紝涓嶈兘娌夌Н婧惰В閾濓紝鑰?/span>AT1.7 PA鍒欒〃鐜板嚭姝ｅ父鐨勬矇縐憾瑙ｉ摑鐨勬ц兘錛涘皢涓ょ鐢?shù)瑙ｈ川鍒嗗埆缁勮閾濈?/span>-澧ㄧ數(shù)姹狅紝AT1.7鍦ㄦ毚闇蹭簬絀烘皵鍚庣粍瑁呯殑鐢墊睜鍑犱箮娌℃湁瀹歸噺錛岃?/span>AT1.7 PA浠嶇劧鍙互姝ｅ父鍏呮斁鐢?shù)锛岃鏄?/span>AT1.7 PA鍏鋒湁浣庢按鍒嗘晱鎰熸с?/span>


鍥?/span>5.錛?/span>a錛?/span>AT1.7 PA涓庯紙b錛?/span>AT1.7緇勮綰芥墸閾?/span>-鐭沖ⅷ鐢墊睜鐨勫驚鐜ц兘

鍥?/span>6.錛?/span>a錛?/span>AT1.7 PA涓庯紙b錛?/span>AT1.7緇勮綰芥墸閾?/span>-鐭沖ⅷ鐢墊睜寰幆鍚庣殑鐢墊睜澹崇収鐗?/span>


  鍙互鐪嬪嚭AT1.7 PA鎵緇勮鐨勭航鎵ｉ摑-鐭沖ⅷ鐢墊睜鍙互姝ｅ父鍏呮斁鐢?shù)弩@鐜紝鑰?/span>AT1.7緇勮鐨勭航鎵ｉ摑-鐭沖ⅷ鐢墊睜鍦ㄥ嚑涓驚鐜悗鍒欎笉鑳藉厖鏀劇數(shù)銆傚垎鍒皢綰芥墸鐢墊睜鎷嗗紑錛屽彲浠ョ湅鍑猴紝浣跨敤AT1.7 PA鐨勭航鎵ｇ數(shù)姹犲嚑涔庢病鏈夎厫铓鐥曡抗錛岃屼嬌鐢?/span>AT1.7鐨勭航鎵ｇ數(shù)姹犺厫铓杈冧負(fù)涓ラ噸錛屽彲瑙佸嚌鑳惰兘澶熸姂鍒舵紡娑茶厫铓銆?/span>

鍥?/span>7.浣跨敤AT1.7涓?/span>AT1.7 PA 鐢?shù)瑙ｈ川閾?/span>/鐭沖ⅷ鐢墊睜鑷斁鐢墊ц兘瀵規(guī)瘮


  灝?/span>AT1.7涓?/span>AT1.7 PA鐢?shù)瑙ｈ川鍒嗗埆缁勮閾?/span>-鐭沖ⅷ鐢墊睜騫跺皢鍏跺厖婊＄數(shù)錛屾悂緗?/span>100涓皬鏃跺悗錛屼嬌鐢ㄤ袱縐嶇數(shù)瑙ｈ川鐨勯摑-鐭沖ⅷ鐢墊睜寮璺數(shù)鍘嬪垎鍒“鍑忓埌1.84 V鍜?/span>2.15 V銆傝鍑濊兌榪樺叿鏈夋姂鍒墮摑紱誨瓙鐢墊睜鑷斁鐢電殑鎬ц兘銆?/span>


  鐩稿叧閾炬帴
  https://doi.org/10.1021/acsami.1c05476
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